Ikizamini cya F-5

Ikizamini cya F-5

Uburyo bwo gukoresha ibikoresho byo gupima fluor / gusesengura ibintu bya fluor:

1. Guhuza ibikoresho Huza inlet ya flask ya distillation kumunwa wo hejuru wa rotameter hamwe numuyoboro wa silicone, uhuze isohoka rya flask ya disillation hamwe ninjoro yigituba cya distillation numuyoboro wa silicone, hanyuma uhuze isohokero ryumuyoboro wa distillation kumunwa wo hejuru wumuyoboro wa condenser hamwe na silicone umuyoboro kugirango uhuze.nozzle y'amazi ihujwe no gusohoka kwa pompe y'amazi akonje, impera yo hepfo y'umuyoboro wa kondenseri ihujwe n'amazi yo mu mazi, naho impera yo hejuru y'umuyoboro wa kondenseri ihuzwa n'amazi.Kuramo icyuma gishyushya, uhuze umugozi w'amashanyarazi, banza winjize icyuma gipima ubushyuhe bwa capillary muri reberi, hanyuma ushyire icyuma muri flask.Kuramo inkoni ndende ya thermostat, uhuze sensor nu bikoresho byerekana ibyuma hanyuma ubishyire mu gipfukisho cy'itanura ry'amashanyarazi.Kuri iyi ngingo, igikoresho kirahujwe.

2. Gukuramo ibikoresho: Ongeramo 900 mL yamazi mumashanyarazi kugirango ufunge icyuma gishyushya, shyira mL 5 ya distillate mumiyoboro ya quartz distillation, hanyuma uhuze imiyoboro yose ya silicone.

3. Gufungura Mbere yo gufungura imashini, banza urebe niba hari amazi akonje hanze, shyiramo icyuma cyamashanyarazi mugikoresho, fungura amashanyarazi, fungura amazi akonje, urebe niba umuyoboro wa kondensate wuzuye ya kondensate kandi igomba gusubira mu kigega cy'amazi.Shyira ubushyuhe bugenzurwa na thermostat kugeza kuri 250 ℃, fungura icyuma gishyushya hamwe na pompe yumuyaga, hanyuma uhindure ubushyuhe bwisaha kugirango ushireho ubushyuhe kuri 110 ℃.Amazi amaze gutekesha flask yatetse, hindura ubushyuhe bwa knob ku isaha kugirango ugumane amazi hafi 85 ℃.Nibyo, hindura metero ya gazi, ugenzure umuvuduko wa gazi kugeza 100 ─ 150 mL / min, hanyuma ugabanye iminota 2 Nyuma yisaha, urebe niba hari distillate itonyanga mumiyoboro ya kondenseri.Niba ihari, nibisanzwe.Niba atari byo, nyamuneka reba niba umuyoboro uhujwe neza kandi amashanyarazi ashyushye ahujwe neza.

4. Kuzimya Urukurikirane rwo guhagarika ni: kuzimya ubushyuhe─ kuzimya pompe yumuyaga─ kuzimya pompe yamazi akonje─ kuzimya amashanyarazi─kuramo amashanyarazi.

gusesengura ibintu bya fluor Kubungabunga metero ya fluor:

1. Gusiga bigomba gukorwa hakurikijwe ibice byasizwe hamwe nuburyo bwo gusiga mbere yo gutangira imashini.

2. Gusenya no guterana ninzobere zumva imiterere yimashini yipimisha.

3. Iyo imashini yipimisha idahari igihe kinini, igomba gushyirwaho amavuta yo kurwanya ingese hejuru yumurimo kandi ikabikwa ahantu humye.

4. Sukura imashini yipimisha.

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Mbere: Laboratoire Ihoraho Ubushyuhe hamwe na Digital Controller

Ibikurikira: Furuka ivu Ibigize Ibizamini

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